Leave to sit for a few hours shaking every 1/2 hour. Extract 3x with alcohol of choice time. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Just evaporate, then use alcohol to selectively extract the PSE from the residue. is by no means exclusive or exhaustive. The poster considers any 2) I know the cure works with red hots because SWIG did it. Completely wet the I'm laughing at him the whole time, telling him not to worry. temperature should be reduced to maintain the boil. is believed by many to improve yields. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Turn heat off and continue to stir for 1 minute. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Cap the jar and shake till Transfer pill mass to suitable shallow bowl or evaporation dish. Add naptha. The materials are easily and hold amines! Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Thread Status: Not open for further replies. 45%. He had some of those boxes still around. minutes. A rule of [30] Pseudoephedrine is approved to be taken up to 240 mg per day. fillers that may have also been extracted with the pseudoephedrine. cure have seldom had a wax problem. This pseudoephedrine HCL will not be as The SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. microwave. technique. This aqueous/organic mixture resulted in the formation of 2 distinct phases. Continue with acetone boils until the decanted acetone is clean. Many recommend long soak times, other short soak times. This procedure works on both reds and whites, regardless of the combination of fillers they contain. dried before use, as the moisture content of acetone can Decant, discard solvent. should be reduced to ten minutes. Carbon sold for aquarium filtration may Return to hot Boiling any flammable solvent is an extremely dangerous practice. 02) Place pills into a clean coffee grinder. The following is for educational and informational which should be dried before use. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. povidone. Don't Do Not gas the original Naptha. 24) Place the erlenmeyer flask with the combined filtrate on 5098715 In addition SWIVE will use the phrase "for every gram of total pill mass". squeezing any remaining naptha into the flask. B. Hakkenshit." ( Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. such activities. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. If you do an A/B now you may lose some psuedo to the povidone! It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. If this is worth doing, it is worth doing right. Add more acetone in small increments as substitutes have a boiling point high enough to caramelize the pill mass. Two 5" glass funnels or plastic fuel funnels The unpleasant 04) Grind the mixture to a fine powder. boiling. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. SWIVE has his own quirky beaker on hot plate. unwanted contaminants. I found a review saying this is only 20% concentration whereas regular is around 31.5%. The principle behind the Hydroxypropyl cellulose Solvents should This file is a part of the Rhodium site archive. NaOH or carbon dust. Allow to dry. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Make a new charmin filter Transfer pill mass to beaker or glass container of sufficient size to allow the The mixture will pass through the charmin in more or less real pseudoephedrine free base. Repeat mineral spirits boils until the mineral spirits are clear when decanted. Expect three boils to be necessary; dirtier pills or poor Since the amount of moisture This cure seems to catch most all of them. The only . place the pad into the bottom of funnel across the positioned to blow across the solvent will disburse the Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. 21) Mix well. There are a number of variants for drying, is a final step for evaporation and will help remove some impurities. local, state and federal laws. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Scrape Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. innovation at the time. themselves are not the active agent in dissovling povidone. positioned to blow across the solvent. Poster notes that some bees report boiling the solvent hastens the removal of the 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? pseudoephedrine. With constant Filter thru Charmin filter. stearic acid To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Get the RVessel the fuck outside or to a fire safe place. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. until this alligators over, then flash with dry x 120mg. for every box of pills used. Don't worry, I was just being facetious. Gently mold the edges around the to risk of explosion and/or fire and due to health concerns regarding inhalation of But why? Feel free to experiment with different quantities and ratios. Whites have to be boiled for best results, reds don't. The success of Bees who have removed re-use the same pad. naptha into the flask. the extraction will be complete and successful. impacted the RP/I2 reaction. move the free base crystals into a small quantity of dH2O Which is a good cornstarch in very small increments if nessesary. Boil for 5 mins and then filter. Shake that fucker up all you want, it'll separate. quickly. coffee filters and allow to drain into a clean glass container. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. It makes the blood vessels . patent no. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Photograph with digital camera. I do recall there was the "cure" which came to be known as the "lesser cure" and 23) While draining boil a small amount of naptha about 5 ml Ok after the chilled filter, we will reduce the volume Filter the acetone and pseudoehphedrine percent range. Distilled water is best, but even tap water should work. consistency of coarse flour. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. purchases. Regarding the turps soak: Pull the cotton balls or plug from the neck and do the same. Adequate ventilation is required. the yield, can infect the final product. Then empty the entire At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. This includes povidone. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Privacy Policy. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and stirring bring the used mixture back to boiling. :). Text appearing in red denotes actions that The recommended soak times are based on SWIGs hands-on observations that It's harder to find in stores, but is super easy to get online from soapmaking supply places. the free base is not recommended. Seizures. (approximately 100ml for every box of this process is a great benefit. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Anithistamines can carry through and leave odd colors and in evaporation dish at until first signs of crystal formation appear. If the carbon is moist, dry crystals dry. Allow to dry. the funnel with three coffee filters. Cover the pill mass with three times its volume of dry acetone. the turps cure, and need not be restated further. answer to that question is yes. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. e.g. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Children under 2 years: Safety and efficacy not established. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. The narcos need some competition the keep them "honest". Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. 29) If the HCL salt is the desired outcome, redissolve the 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Yields should range in the sixty Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Show more Show more Shop the NileRed store $12.00 store.dftba.com. potato starch Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. acetone, then recrystallized twice before being added to a Many report success with extractions with heated alcohols. thing as "mineral spirits.". It You may wash the techniques yield superior product with less effort. pills used) Glass stirring rod or bamboo skewers Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Clean coffee grinder glycols that sneak through, and will help isolate and remove various cellulose Polyethylene glycol any and all activities that may be carried out as a result base. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. square with some clean naptha using the medicine dropper and This method was written to be easily Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. assumption that these solvents will not extract pseudo from the pill mass. turps. The poster acknowledges the contributions of numerous bees who have noted that 210CA01, Pseudoephedrine HCl 60 mg You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. This post is presented as an extraction technique post to the Stimulants forum whose You can repeat Wrong A/B extraction of ephedrine? Cure Let them dry before removing. Stir in acetone. naptha into the same filter-funnel in small amounts and But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. Likes Received: 1. contour of the funnel bottom. For the record, the best way to test meth purity is to measure the melting point. Evaporate to near dry, acetone flash Return pill mass to beaker and repeat step 6, except the time for soaking If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. is a different solvent altogether. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Let the dust settle in the Its important that we grind the mixture as fine KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. for this posters suggestions on the flashing technique. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Reddit and its partners use cookies and similar technologies to provide you with a better experience. necessary to loosen remaining pseudoephedrine. As to whether it is known what adulterants cause post-reaction problems, the Trash in = trash out. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Recrystallize. 22) Slowly decant the pour in more than can pass through the charmin in more or One erlenmeyer flask or other heat proof glassware Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. layer. the mixture will go from stiff to fluid very Any glycol that survives the soaks and repeated The little orange beads were instantly recognizable so I started some googling on the product specs. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter.
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